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020 _a0471607118
037 _cTextbook
040 _aCSL
_beng
_cCSL
041 _aeng
084 _aC216-53:8 K81;M9 TE
_qCSL
100 _aStout, George H
_eauthor
_9719956
245 0 _aX-ray structure determination : a practical guide
250 _a2nd ed.
260 _aCanada :
_bWiley,
_c1989.
300 _axv, 453p.
_b: ill.
500 _aAppendixes 421-440p.; Index 441-453p.
520 _aClosely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
650 _a Crystals
_9815836
650 _a Patterson methods
_9815837
650 _aDerived results
_9815838
700 _aJensen, Lyleh H
_eco-author
_9815839
942 _hC216-53:8 K81;M9 TE
_cTB
_2CC
_n0
999 _c7673
_d7673